Videos

In-service lubricant testing laboratories are faced with increasing demands for profitability and customer satisfaction. To help support these goals, an innovative oil analysis methodology is now available.  Regular testing for fuel and glycol in used engine oil by gas chromatography can provide guidance on oil handling. Benefits include: Prevention of unnecessary oil changes  Lowered costs associated with enhanced replaceable fluid lifetime  Advanced warning of component wear...

Volatile organics like naphtha are amongst the most challenging samples to be analyzed by ICP techniques. Wealth of emission lines originating from the organic matrix and high volatility demonstrate challenges for ICP-OES analyzers. A robust plasma as well as an optical system with high spectral resolution are required in order to routinely quantify trace elements in the low µg/kg range. For specification analysis in the low µg/kg range ICP-MS often is the method of choice as conventiona...

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Over the past 20 years, advances in modern ultra-high resolution mass spectrometry have forever changed the expectations of petroleum analyses. Facilitated by advances in ionization methods (that enable molecular-level analysis irrespective of initial or final boiling point), ultra-high resolution Fourier Transform Ion Cyclotron Resonance mass spectrometry (FT-ICR MS) routinely resolves and identifies tens-of-thousands of species (at the level of elemental composition assignment) in individua...

Being a founding member of the Allotrope Foundation - granted the 2017 Bio-IT World Best Practice Award in Knowledge Management - Bayer is implementing strategically the Allotrope Framework to escort scientific data throughout its complete lifecycle from method development over acquisition, processing, reporting, archiving to submission, using a common set of standard tools. Allotrope aims to make the intelligent analytical laboratory a reality – an automated laboratory where data, methods...

Oil industry started long before 1900 and is older than gas chromatography, so test distillation was used for sample analysis and not GC. Fast GC analysis of Diesel and Jetfuel already is a standard but Gasoline is not. Detailed hydrocarbon analysis (DHA) with pattern recognition uses GC analysis input to separate and identify gasoline and blendfeed compounds in 6 minutes. The composite report of DHA is input for the fugacity filmmodel of ASTM method D86 distillation. GC post-run software all...

Non-traditional gasoline additives (NTGAs) like ethyl acetate are being researched as beneficial octane-booster replacements for ethanol and methyl tert-butyl ether. Other octane-enhancing NTGAs, including acetone and N-methylaniline which can degrade automobile engine performance, are sometimes used illegally in gasolines outside the United States and Europe. Unfortunately, monitoring programs relying on ASTM D6730 (Detailed Hydrocarbon Analysis) and ASTM 6839 (Multidimensional Gas Chromatog...

Today's quality control labs face high regulatory and financial pressures. International and national regulations (e.g. ASTM D6667, D5453, D5762, D7457 etc.), set high standards for the labs and especially in industry and contract labs - analysis has to be affordable in order to keep a competitive pricing for final products and offered services. Additionally, complex sample matrices make even routine S/N/Cl/C determinations difficult and the amount of samples that have to be analyzed in th...

The petrochemical and chemical industries are facing new challenges. Extended focus, new legislation, regulations and better standards have been presented by governments and regulators for air quality management. New solutions are now required to provide high sensitivity, low detection limit, continuous and spatial monitoring as a real time control and prevention tool for fugitive emissions. In order to meet these challenges, automation of remote sensing technology based on Open-Path FTIR...

Heavy Fuel Oil (HFO) is the most widely used marine fuel at this time and only a comparable small part is used for oil-fired power plants. It is derived from the residue after crude oil distillation and is characterized by a high viscosity, and requires heating for storage, pumping and burning. A critical factor is the high amount of e.g. sulfur and other heteroatomic compounds. Because of environmental and health implications the limits for e.g. sulfur has decreased constantly from max. 1.5%...